HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylallylamine → HCID 178457238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylallylamine | HCID 69391 | — |
| Reactant | HCID 178484053 | HCID 178484053 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178457238 | HCID 178457238 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-N-[4-(4-bromo-(E)-but-2-enyloxymethyl)-cyclohexylmethyl]-N-methyl-4-trifluoromethyl-benzenesulfonamide was reacted with N-allyl-methyl-amine in N,N-dimethylacetamide at room temperature to yield trans-N-{4-[4-(allyl-methyl-amino)-(E)-but-2-enyloxymethyl]-cyclohexylmethyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide as light yellow viscous oil, MS: 489 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-a2ef48ca991d47c59183689d6c9dee27 |
| Source note | uspto-grants-2005_10 |