HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 178484065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | HCID 178484052 | HCID 178484052 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178484065 | HCID 178484065 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-[4-(4-bromo-butoxymethyl)-cyclohexylmethyl]-methyl-carbamic acid 4-chloro-phenyl ester was reacted with bis-(2-hydroxy-ethyl)-amine in N,N-dimethylacetamide at 50° C. for 3 hours to yield trans-(4-{4-[bis-(2-hydroxy-ethyl)-amino]-butoxymethyl}-cyclohexylmethyl)-methyl-carbamic acid 4-chloro-phenyl ester as colorless viscous oil, MS: 471 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-4f6d1ee35af74c639e01f9db1255a13a |
| Source note | uspto-grants-2005_10 |