HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10128150, compound → HCID 86601097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10128150 | HCID 10128150 | — |
| Reactant | HCID 22311322 | HCID 22311322 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86601097 | HCID 86601097 | — |
Reaction Steps
Prepared from 7-Chloromethyl-chromen-2-one and starting compound A1 as described for compound 11. After the addition of water, the mixture is extracted with diethyl ether. The ether solution is dried over magnesium sulfate. After the addition of a saturated solution of hydrochloric acid in ether, the compound precipitates. M. p. 264-267° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953853B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-67b317b5dbb243cfaa1e15855ec3c082 |
| Source note | uspto-grants-2005_10 |