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HRID967436

反应详情

EQUATION

反应方程式

HRID 967436 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CN(C)C=NS(=O)(=O)c1ccccc1-c1ccc(CN)cc1
HCID69652288

未命名化合物

PRODUCTS

生成物

1
结构：Cl.NCc1ccc(-c2ccccc2S(N)(=O)=O)cc1
HCID69652290

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

400 mg of 4′-Aminomethyl-biphenyl-2-sulfonic acid dimethylaminomethyleneamide were treated with 10 ml MeOH and 4 ml conc. HCl and refluxed for 1 h. Solvent and HCl were evaporated and the product used without purification.

WORKUP

后处理

  1. temperaturerefluxed for 1 h
  2. customSolvent and HCl were evaporated
  3. customthe product used without purification