HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178510197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 178453094 | HCID 178453094 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178510197 | HCID 178510197 | — |
Reaction Steps
To a solution of 500 mg (2′-Hydroxy-3,4,5,6-tetrahydro-2H-[1,4′]bipyridinyl-4-ylmethyl)-carbamic acid tert-butyl ester in 5 ml CH2Cl2 3 ml TFA was added dropwise at 0° C. After 16 h 20 ml toluene were added and the solvent removed under reduced pressure to yield a brown foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953857B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-bb4ff88136124a5e9d8a4869e5dd8446 |
| Source note | uspto-grants-2005_10 |