Hydrochloric Acid → HCID 178487770, compound

Participants

Reaction Steps

A mixture of the product from Step A (10.5 g, 48 mmol), water (250 mL), and conc HCl (2.5 mL) was refluxed for 30 min. The volume of the reaction mixture was reduced by evaporation (ca 100 mL) and the pH adjusted to 7 by the slow addition of a saturated aqueous solution of sodium carbonate at room temperature. The solid that formed upon standing was collected and dried to give a gray solid (6.8 g): APCl/LCMS m/z 165 (M+H)+.

Provenance & Evidence