2-Chlorobenzenesulfonamide → HCID 22291403, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 18 from phenyl 2-{4-[4-phenyl-2-(trifluoromethyl)-1H-imidazol-1-yl]phenyl}ethylcarbamate and 2-chlorobenzenesulfonamide. MS (ESI) m/z 549 [M+H]+, 547 [M−H]−, 1H-NMR (CDCl3) δ 2.86 (2H, t, J=7.3 Hz), 3.48-3.55 (2H, m), 6.58 (1H, br), 7.25-7.28 (1H, m), 7.31-7.36 (3H, m), 7.25-7.28 (1H, m), 7.39-7.47 (4H, m), 7.58-7.61 (2H, m), 7.82 (2H, dd, J=8.4, 1.4 Hz), 8.00 (2H, d, J=7.5 Hz).

Provenance & Evidence