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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 967996Generated: November 1, 2026

Sodium borohydride → HCID 69587603, compound

https://huagongshe.com/reaction/967996

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 86584324HCID 86584324—
SolventMethanolHCID 887—
ProductHCID 69587603HCID 69587603—

Reaction Steps

A mixture of 4-[4-(1-Ethyl-propylamino)-3,6-dimethyl-pyridin-2-yloxy]-3,5-dimethyl-benzaldehyde and sodium borohydride in methanol was stirred at room temperature. After standard work-up procedure and purification, the title compound was obtained as a solid. 1H NMR(CDCl3) d 7.06(s, 2H), 6.08(s, 1H), 4.64(s, 2H), 3.74(d, 1H), 3.33(m, 1H), 2.14(s, 3H), 2.13(s, 3H), 2.11(s, 6H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06956047B1
Source datasetuspto-grants-2005_10
ORD IDord-b1beaddef4904cb3b635962a1827fd08
Source noteuspto-grants-2005_10