HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 69587603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86584324 | HCID 86584324 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69587603 | HCID 69587603 | — |
Reaction Steps
A mixture of 4-[4-(1-Ethyl-propylamino)-3,6-dimethyl-pyridin-2-yloxy]-3,5-dimethyl-benzaldehyde and sodium borohydride in methanol was stirred at room temperature. After standard work-up procedure and purification, the title compound was obtained as a solid. 1H NMR(CDCl3) d 7.06(s, 2H), 6.08(s, 1H), 4.64(s, 2H), 3.74(d, 1H), 3.33(m, 1H), 2.14(s, 3H), 2.13(s, 3H), 2.11(s, 6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956047B1 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-b1beaddef4904cb3b635962a1827fd08 |
| Source note | uspto-grants-2005_10 |