Glyoxylic Acid → HCID 85800996, compound

HRID 968146Notes

Reaction equation

HRID 968146 reaction equation
[C:1]([OH:5])(=[O:4])[CH:2]=O.[CH3:6][C:7](=[O:19])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>P(=O)(O)(O)O>[CH2:9]([C:8]([C:7](=[O:19])[CH3:6])=[CH:2][C:1]([OH:5])=[O:4])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 2

HCID 760Glyoxylic AcidHCID 116222-Tridecanone

Product 1

HCID 85800996HCID 85800996, compound

Reagents, catalysts & solvents 1

HCID 1004Phosphoric AcidSolvent

Procedure

Prepared from glyoxylic acid (4.94 g, 6.5 mmol), 2-tridecanone (12.9 g, 6.5 mmol) and orthophosphoric acid (20 ml). 1H n.m.r. δ (CDCl3) 0.87, t J 7.2 Hz, 3H, CH3; 1.30, m, 16H, CH2; 2.39, s, 3H, CH3; 2.77, t J 7.0 Hz, 2H, CH2; 6.50, s, CH.

Sources & evidence

ORD record
ord-7384c12a0e404fd4bb5b08590bc12de6
Source dataset
uspto-grants-2005_10
Patent number
US06958145B2

Reaction notes

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