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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 968146Generated: October 29, 2026

Glyoxylic Acid → HCID 85800996, compound

https://huagongshe.com/reaction/968146

Reaction equation

Participants

RoleNameHCIDCharge
ReactantGlyoxylic AcidHCID 760—
Reactant2-TridecanoneHCID 11622—
SolventPhosphoric AcidHCID 1004—
ProductHCID 85800996HCID 85800996—

Reaction Steps

Prepared from glyoxylic acid (4.94 g, 6.5 mmol), 2-tridecanone (12.9 g, 6.5 mmol) and orthophosphoric acid (20 ml). 1H n.m.r. δ (CDCl3) 0.87, t J 7.2 Hz, 3H, CH3; 1.30, m, 16H, CH2; 2.39, s, 3H, CH3; 2.77, t J 7.0 Hz, 2H, CH2; 6.50, s, CH.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06958145B2
Source datasetuspto-grants-2005_10
ORD IDord-7384c12a0e404fd4bb5b08590bc12de6
Source noteuspto-grants-2005_10