HRID968171

反应详情

EQUATION

反应方程式

HRID 968171 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

An aqueous solution prepared by dissolving 4-methylphenylbenzylpiperidinium bromide (13.85 g, 0.04 mmol) in 20 ml of deionized water was mixed with an aqueous solution prepared by dissolving potassium hexafluorophosphate (KPF6, 8.83 g, 0.048 mmol) in 30 ml of deionized water and the produced white solid was collected by filtration. The resulting white solid was washed with 300 ml of deionized water, subjected to filtration and dried to obtain 4-methylphenylbenzylpiperidinium hexafluorophosphate (15.6 g, yield: 95%).

WORKUP

后处理

  1. customAn aqueous solution prepared
  2. additionwas mixed with an aqueous solution
  3. customprepared
  4. filtrationthe produced white solid was collected by filtration
  5. washThe resulting white solid was washed with 300 ml of deionized water
  6. filtrationsubjected to filtration
  7. customdried