HRID968171
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
An aqueous solution prepared by dissolving 4-methylphenylbenzylpiperidinium bromide (13.85 g, 0.04 mmol) in 20 ml of deionized water was mixed with an aqueous solution prepared by dissolving potassium hexafluorophosphate (KPF6, 8.83 g, 0.048 mmol) in 30 ml of deionized water and the produced white solid was collected by filtration. The resulting white solid was washed with 300 ml of deionized water, subjected to filtration and dried to obtain 4-methylphenylbenzylpiperidinium hexafluorophosphate (15.6 g, yield: 95%).
WORKUP
后处理
- customAn aqueous solution prepared
- additionwas mixed with an aqueous solution
- customprepared
- filtrationthe produced white solid was collected by filtration
- washThe resulting white solid was washed with 300 ml of deionized water
- filtrationsubjected to filtration
- customdried