Potassium hexafluorophosphate → 4-Methylphenylbenzylpiperidinium hexafluorophosphate

Participants

Reaction Steps

An aqueous solution prepared by dissolving 4-methylphenylbenzylpiperidinium bromide (13.85 g, 0.04 mmol) in 20 ml of deionized water was mixed with an aqueous solution prepared by dissolving potassium hexafluorophosphate (KPF6, 8.83 g, 0.048 mmol) in 30 ml of deionized water and the produced white solid was collected by filtration. The resulting white solid was washed with 300 ml of deionized water, subjected to filtration and dried to obtain 4-methylphenylbenzylpiperidinium hexafluorophosphate (15.6 g, yield: 95%).

Provenance & Evidence