Hydrochloric Acid → 6059-44-5

HRID 968374Notes

Reaction equation

HRID 968374 reaction equation
[ClH:1].[NH2:2][CH:3]([CH2:7][NH2:8])[C:4]([OH:6])=[O:5].Cl.[CH3:10]O>>[ClH:1].[ClH:1].[CH3:10][O:5][C:4](=[O:6])[CH:3]([NH2:2])[CH2:7][NH2:8]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 1086382,3-Diaminopropionic acid hydrochloride

Product 1

HCID 136429026059-44-5

Conditions

Temperature
0 °C

Procedure

2,3-Diaminopropionic acid monohydrochloride (2.0 g, 14.3 mmol) is suspended in dry methanol (80 ml) and cooled on 0° C. Dry HCl gas is introduced into the solution for 30 min. Stirring is carried out at room temperature for 48 h, and the solvent is then removed in vacuo. The desired compound is obtained as a colorless solid and used directly for the next reaction.

Workup

  1. customthe solvent is then removed in vacuo

Sources & evidence

ORD record
ord-20924baf721b4672ba2eea4a80bb2dc7
Source dataset
uspto-grants-2005_10
Patent number
US06958395B2

Reaction notes

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