Nitrogen → N,N'-Dicyclohexylurea

Participants

Reaction Steps

By mixing 0.1 g of polymer coupling agent from step 2, 0.15 g of 1,3-dicyclohexylcarbodiimide (DCC) in 2 g of THF, a 5 wt % polymer coupling agent solution is prepared. 20 μL of triethylamine is added into the mixture. The solution is then pumped into the capillary by N2 pressure. After 3 drops of the initiator solution come out of the other end of the capillary, both ends of the capillary are sealed with a silicon rubber septum. The reaction is allowed to proceed for 12.0 hour at room temperature. The capillary is then rinsed with acetone for 1.0 hour.

Provenance & Evidence