Water → HCID 86590095, compound

Participants

Reaction Steps

The 2-bromoacetophenone of 4.97 g (0.025 moles) was dissolved in nitromethane of 9.5 g. Tetrahydrothiophene of 2.2 g (0.025 moles) was added at room temperature, and was matured as it is for two hours at room temperature. A reaction liquid was hardened by the progression of reactions. Solids were dissolved by adding 70 g of water and 50 g of diethyl ether. A water layer was separated and washed with 50 g of diethyl ether of 50 g so that lipophilic impurities were removed.

Provenance & Evidence