Azobisisobutyronitrile → HCID 86605409, compound

Participants

Reaction Steps

2.0 g of methylmethacryilic acid, 9.0 g of t-butylacrylate, 1.0 g of maleic anhydride, 1.2 g of N-[(perfluorooctanesulfonyl)oxy]-norbornene-2,3-dicarboximide and 0.5 g of AIBN were dissolved in 50 g of acetone. The monomers were polymerized at 67° C. for 6 hours. After completion of the polymerization, the polymerized product was precipitated in water, filtered, and dried in a vacuum to give poly(methylmethacrylic acid-t-butylacrylate-maleic anhydride-N-[(perfluorooctanesulfonyl)oxy]-norbornene-2,3-dicarboximide) in a yield of 78%. The structure of the polymer was identified by 1H-NMR spectroscopy (FIG. 1).

Provenance & Evidence