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HRID968536

反应详情

EQUATION

反应方程式

HRID 968536 的结构方程式

REACTANTS

反应物

3
结构：O=C(Cl)c1ccccc1
HCID7412

Benzoyl chloride

C7H5ClO

结构：N.N#CS
HCID13417437

未命名化合物

结构：COc1ccc(C2CCOCC2)cc1N
HCID21919262

2-Methoxy-5-(tetrahydro-2H-pyran-4-yl)benzenamine

C12H17NO2

PRODUCTS

生成物

1
结构：COc1ccc(C2CCOCC2)cc1NC(=S)NC(=O)c1ccccc1
HCID22719571

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

To a solution of ammonium rhodanide in acetone is added benzoyl chloride and a solution of 2-methoxy-5-(tetrahydro-pyran-4-yl)-phenylamine (IX). The reaction is carried out under reflux for about 20 minutes. The product 1-benzoyl-3-[2-methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea (X) is isolated by conventional means.

WORKUP

后处理

  1. temperatureunder reflux for about 20 minutes