HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → 6-(Pyridin-3-yloxy)-hexylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-[6-Amino-1-hexyl-oxy]-pyridine, hydrochloride | HCID 131726699 | — |
| Solvent | Water | HCID 962 | — |
| Product | 6-(Pyridin-3-yloxy)-hexylamine | HCID 23132443 | — |
Reaction Steps
A solution of 3-[6-amino-1-hexyl-oxy]-pyridine, hydrochloride in water was made strongly alkaline with sodium hydroxide and ectracted twice with chloroform. The organic phase was dried and evaporated in vacuo to yield an oil which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07304066B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-400a87ef9ff74a5ebd328dac00c7c395 |
| Source note | uspto-grants-2007_12 |