HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10052201, compound → HCID 10324256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10052201 | HCID 10052201 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10324256 | HCID 10324256 | — |
Reaction Steps
A solution of Example 40 (10 mg) in ethanol (4 mL) was added to 10% palladium on carbon (50 mg) and stirred under 1 atmosphere pressure of hydrogen at 20 degrees for 4 h. Catalyst was removed by filtration and washed with ethanol (10 mL). Filtrate and washings were combined and solvent was removed to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07304087B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-45d77f471e6f4d698a46d8710f5d3463 |
| Source note | uspto-grants-2007_12 |