Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 969434Generated: October 31, 2026

Sodium Iodide → HCID 68908797, compound

https://huagongshe.com/reaction/969434

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium IodideHCID 5238—
ReactantDimethylformamideHCID 6228—
ReactantPotassium CarbonateHCID 11430—
Reactant3-Pentyl-8-azabicyclo[3.2.1]octaneHCID 21989852—
ProductHCID 68908797HCID 68908797—

Reaction Steps

Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63)(0.094 g), 3-pentyl-8-azabicyclo[3.2.1]octane (0.027 g, 0.15 mmol), NaI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c5)(0.025 g). HPLC-MS (ammonium acetate) [M+H]+=383.34

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07307075B2
Source datasetuspto-grants-2007_12
ORD IDord-e55c3ebaf5214187804852dcf365d2c4
Source noteuspto-grants-2007_12