HRID969463

反应详情

EQUATION

反应方程式

HRID 969463 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

306 mg (0.6 mmol) 8-benzyloxy-5-{1-hydroxy-2-[2-(4-methoxy-phenyl)-1,1-dimethyl-ethylamino]-ethyl}-1H-quinolin-2-one are dissolved in 10 mL methanol and hydrogenated with palladium on charcoal as catalyst at ambient temperature and normal pressure. Then the catalyst is separated off and the filtrate is freed from the solvent.

WORKUP

后处理

  1. customThen the catalyst is separated off