HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69462583, compound → HCID 11531056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69462583 | HCID 69462583 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11531056 | HCID 11531056 | — |
Reaction Steps
306 mg (0.6 mmol) 8-benzyloxy-5-{1-hydroxy-2-[2-(4-methoxy-phenyl)-1,1-dimethyl-ethylamino]-ethyl}-1H-quinolin-2-one are dissolved in 10 mL methanol and hydrogenated with palladium on charcoal as catalyst at ambient temperature and normal pressure. Then the catalyst is separated off and the filtrate is freed from the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07307076B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-dd736a9fb4884813b26c9d91eba5ceee |
| Source note | uspto-grants-2007_12 |