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HRID969604

反应详情

EQUATION

反应方程式

HRID 969604 的结构方程式

REACTANTS

反应物

2
结构：c1ccc2[nH]ccc2c1
HCID798

Indole

C8H7N

结构：CC(C)c1cc(C(C)C)c(S(=O)(=O)Cl)c(C(C)C)c1
HCID81042

2,4,6-Triisopropylbenzenesulfonyl chloride

C15H23ClO2S

PRODUCTS

生成物

1
结构：CC(C)c1cc(C(C)C)c(S(=O)(=O)n2ccc3ccccc32)c(C(C)C)c1
HCID11303634

未命名化合物

收率 88%

PROCEDURE

实验过程

The title compound was prepared from 2,4,6-triisopropyl-benzene sulfonyl chloride and 1H-indole, according to Method A, described above. Yield 88%; mp 131-133° C.; 1H NMR (CDCl3) δ 7.41-7.65 (m, 3H), 7.18-7.28 (m, 4H), 6.65-6.68 (dd, J=8 Hz, 1H), 4.15-4.31 (m, 2H), 2.81-2.97 (m, 1H), 1.28 and 1.29 (2s, 6H), 0.98-1.12 (m, 12H).