Hydrochloric Acid → HCID 10451932, compound

Participants

Reaction Steps

N-(1-Acetyl-3,3-dimethyl-2,3-dihydro-1H-indol-6-yl)-2-[(pyridin-4-ylmethyl)-amino]-benzamide (Example 2, 120 mg) was heated with HCl (5 N, 2.5 mL) and H2O (2.5 mL) to reflux for 2 h. The solvent was evaporated and the residue was washed with MeOH. The desired compound was collected after filtration as an off-white solid. MS: (ES+) 373 (M+H). Calc'd. for C23H24N4O-372.20.

Provenance & Evidence