HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 969713Generated: November 4, 2026
Isoamyl Nitrite → HCID 86598711, compound
https://huagongshe.com/reaction/969713
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 85871668 | HCID 85871668 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86598711 | HCID 86598711 | — |
Reaction Steps
9-Acetyl-2-amino-6-iodopurine (1.44 g, 4.72 mmol), bromotrimethylsilane (2.17 g, 14.2 mmol) and isoamyl nitrite (0.83 g, 5.67 mmol) were added to tetrahydrofuran (5 ml), and the mixture was stirred 20-25° C. for 19 hr to give 2-bromo-6-iodopurine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07307167B2 |
|---|
| Source dataset | uspto-grants-2007_12 |
|---|
| ORD ID | ord-5cd26d9d638a4514b63677a393bef6e2 |
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| Source note | uspto-grants-2007_12 |
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