HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 178442569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 131726714 | HCID 131726714 | — |
| Reactant | HCID 178418311 | HCID 178418311 | — |
| Product | HCID 178442569 | HCID 178442569 | — |
Reaction Steps
A mixture of 14.0 g (0.17 mol) of 3-amino-1,2,4-triazole, 51.7 g (0.17 mol) of 3-oxo-2-octyl-4-phenylbutanoate and 3. g of p-toluenesulfonic acid was heated under reflux for 6 h. Work-up was carried out analogously to Ex. 1. Drying gave 37 g (0.11 mol) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07307172B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-ff1917b825a94183b4531878754fc450 |
| Source note | uspto-grants-2007_12 |