HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 59017637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178442569 | HCID 178442569 | — |
| Product | HCID 59017637 | HCID 59017637 | — |
Reaction Steps
A mixture of 17 g (0.05 mol) of 7-hydroxy-6-octyl-5-phenyl-[1,2,4]-triazolo-[1,5-α]-pyrimidine (cf. Ex. 7) and 50 ml of phosphorus oxychloride was heated under reflux for 8 h. Work-up was carried out analogously to Ex. 2. This gave 16 g (0.046 mol) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07307172B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-a3d5d01d958b4868845f4dd922d29a10 |
| Source note | uspto-grants-2007_12 |