Cyclopentylamine → HCID 59017638, compound

Participants

Reaction Steps

With stirring, a mixture of 0.13 g (1.5 mmol) of cyclopentylamine and 0.15 g (1.5 mmol) of triethylamine in 10 ml of methylene chloride was added to a mixture of 0.52 g (1.5 mmol) of 7-chloro-6-octyl-5-phenyl-[1,2,4]-triazolo-[1,5-α]-pyrimidine (cf. Ex. 8) in 20 ml of methylene chloride. The reaction mixture was stirred at room temperature for 16 h, work-up was carried out analogously to Ex. 3. This gave 0.52 g (1.3 mmol) of the title compound (melting point 81° C.).

Provenance & Evidence