HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzoic Acid → HCID 58935106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzoic Acid | HCID 135 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Chloromethyl ethyl ether | HCID 18523 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58935106 | HCID 58935106 | — |
Reaction Steps
36.7 ml (0.26 mole) Of triethylamine were added under a nitrogen atmosphere to a solution of 36.1 g (0.26 mole) of 4-hydroxybenzoic acid in 200 ml of dichloromethane. The mixture was cooled in an ice-water bath, and 24.5 ml (0.26 mole) of chloromethyl ethyl ether in 100 ml of dichloromethane were added dropwise.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07311948B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-f7f2f439edd743b8af62f935d1198322 |
| Source note | uspto-grants-2007_12 |