HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 970246Generated: October 28, 2026
4-Methoxyphenol → HCID 23516352, compound
https://huagongshe.com/reaction/970246
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Reactant | HCID 58935103 | HCID 58935103 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23516352 | HCID 23516352 | — |
Reaction Steps
98.5g (0.2 mole) of ethoxymethyl 4-(4-(6-acryloyloxyhexyloxy)-benzoyloxy)-benzoate (12) were dissolved in 400 ml of ethanol and 5 g (0.02 mole) of pyridinium 4-toluenesulfonate and 20 mg of 4-methoxyphenol were added. The mixture was heated at 60° C. for 15 h. After cooling down to room temperature the product crystallized. It was collected, washed with 300 ml of ethanol, and dried in the desiccator after which 55.3 g of a white powder (67%) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07311948B2 |
|---|
| Source dataset | uspto-grants-2007_12 |
|---|
| ORD ID | ord-9b561dcb938449ffad2e1a2508075605 |
|---|
| Source note | uspto-grants-2007_12 |
|---|
