HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Dimethyl 4-{3-[4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl]propyl}phthalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromopinacolone | HCID 21642 | — |
| Reactant | HCID 17983061 | HCID 17983061 | — |
| Product | Dimethyl 4-{3-[4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl]propyl}phthalate | HCID 17983003 | — |
Reaction Steps
In a manner similar to Example 1g, by reacting 900 mg (2.6 mmol) of dimethyl 4-[3-(3-methyl-4-hydroxyphenyl)propyl]phthalate with 400 mg (2.9 mmol) of potassium carbonate and 390 μl (2.9 mmol) of 1-bromopinacolone. A colorless oil is obtained (m=910 mg; y=79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312249B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-0cd8fa063f6f4ef38c8aae301f58178a |
| Source note | uspto-grants-2007_12 |