HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17983061, compound → 4-[3-(3,4-Bis-hydroxymethyl-phenyl)-propyl]-2-methyl-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17983061 | HCID 17983061 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 4-[3-(3,4-Bis-hydroxymethyl-phenyl)-propyl]-2-methyl-phenol | HCID 69492069 | — |
Reaction Steps
In a manner similar to Example 3a, by reacting 1 g (2.9 mmol) of dimethyl 4-[3-(3-methyl-4-hydroxyphenyl)propyl]phthalate (Example 2e) with 260 mg (7 mmol) of lithium aluminum hydride. A white solid is obtained (m=740 mg, m.p.=92° C., y=89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312249B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-36c7255922574875952f0b20fc474f50 |
| Source note | uspto-grants-2007_12 |