HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 69406753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69408191 | HCID 69408191 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 69406753 | HCID 69406753 | — |
Reaction Steps
This product is obtained according to a procedure identical to that described in example B from 0.8 g (2.61 mmol) of compound 17. Compound 18·4HCl is isolated in the form of an off-white powder. This powder is dissolved in the minimum amount of water and the solution is brought to basic pH by addition of NaOH pellets. After extraction with 3×100 ml of chloroform and drying over MgSO4, the solvents are evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312327B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-450cf6ed6d08457aac53eb3d1abd7dcd |
| Source note | uspto-grants-2007_12 |