HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 59019996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 59020235 | HCID 59020235 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 59019996 | HCID 59019996 | — |
Reaction Steps
A solution of the product from Example 197 (15.0 mg, 0.028 mmol) in 5 ml of 4N HCl in dioxane and 0.5 mL of THF was refluxed for 6 hr. The mixture was cooled to rt and purified with reverse phase HPLC to give the desired product as white solid. MS found: (M+1)+=509.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312214B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-be75cf8759fc47b4bf42f542e8ab2aec |
| Source note | uspto-grants-2007_12 |