HRID971254

反应详情

EQUATION

反应方程式

HRID 971254 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3,3-dimethyl-6-nitroindolin-2-one (500 mg, 2.4 mmol), 10% Pd—C (100 mg), and MeOH (100 mL) was stirred under H2 (1 atm) for 3 h. After that the catalyst was filtered off and the filtrate was concentrated to give an off-white solid (420 mg).

WORKUP

后处理

  1. filtrationAfter that the catalyst was filtered off
  2. concentrationthe filtrate was concentrated