HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → 5-Phenylsulfanyl-indan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Fluoro-1-indanone | HCID 136537 | — |
| Product | 5-Phenylsulfanyl-indan-1-one | HCID 12551992 | — |
Reaction Steps
5-Fluoro-1-indanone from Aldrich Sigma Chemical Co. (Cat No. 18,566-3) was treated with benzenethiol in the presence of potassium carbonate using the procedure of step 4 of Example 1 to afford 5-phenylsulfanyl-indan-1-one. MS: 241 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312359B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-b93039970709431e91d346acbf9702d0 |
| Source note | uspto-grants-2007_12 |