Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 971495Generated: October 30, 2026

HCID 12278206, compound → HCID 178506831, compound

https://huagongshe.com/reaction/971495

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 12278206HCID 12278206—
ReactantButyllithiumHCID 178418339—
ProductHCID 178506831HCID 178506831—

Reaction Steps

By the method described in Example 7 using n-butyl lithium solution (9% w/v, 10 ml, 0.014 mol), and 2-ethyl-5,6,7,8-tetrahydroquinoline (2.3 g, 0.014 mol) and title compound is prepared and converted in situ to methyl 2-ethyl-5,6,7,8-tetrahydroquinoline-8-carboxylate which was converted to the corresponding 8-thioamide by the procedure described in U.S. Ser. No. 460,265.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04160094
Source datasetuspto-grants-1979_07
ORD IDord-6758861bd91c4bdb94082602032be8c9
Source noteuspto-grants-1979_07