HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12278206, compound → HCID 178506831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12278206 | HCID 12278206 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 178506831 | HCID 178506831 | — |
Reaction Steps
By the method described in Example 7 using n-butyl lithium solution (9% w/v, 10 ml, 0.014 mol), and 2-ethyl-5,6,7,8-tetrahydroquinoline (2.3 g, 0.014 mol) and title compound is prepared and converted in situ to methyl 2-ethyl-5,6,7,8-tetrahydroquinoline-8-carboxylate which was converted to the corresponding 8-thioamide by the procedure described in U.S. Ser. No. 460,265.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04160094 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-6758861bd91c4bdb94082602032be8c9 |
| Source note | uspto-grants-1979_07 |