HCID 12278207, compound → HCID 178506830, compound

Participants

Reaction Steps

By the method described in Example 7 using n-butyl lithium solution (9% w/v, 13.5 g, 0.03 mol) and 2-n-butyl-5,6,7,8-tetrahydroquinoline (6 g., 0.03 mol) the title compound is prepared and converted in situ to methyl 2-n-butyl-5,6,7,8-tetrahydroquinoline-8-carboxylate and then to the corresponding 8-thioamide by the procedure described in U.S. Ser. No. 460,265.

Provenance & Evidence