HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 36689053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131709976 | HCID 131709976 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 36689053 | HCID 36689053 | — |
Reaction Steps
3.36 g of Z-Ile-Gly-OMe are dissolved in 100 ml of methanol and 10 ml of 1 N hydrochloric acid and hydrogenated in the presence of 0.5 g of Pd on charcoal (10%). After filtering off the catalyst the solvent is completely evaporated. The resulting foam is homogeneous in a thin layer chromatogram on silica gel; Rf = 0.26 in chloroform-methanol (95:5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159981 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-523a5ec09d394c9da1ad4cac392646df |
| Source note | uspto-grants-1979_07 |