HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20518157, compound → HCID 20518134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20518157 | HCID 20518157 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 20518134 | HCID 20518134 | — |
Reaction Steps
A solution of 4.0 g of the above hydrochloride in 250 ml of 48% hydrobromic acid is stirred and refluxed for two hours. The reaction mixture is evaporated in vacuo to yield 6-chloro-1-(2-bromophenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04160765 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-7c0a5596156c455381eb4e7718e71170 |
| Source note | uspto-grants-1979_07 |