HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 54453186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-(4-Phenoxyphenyl)pyrrolidine | HCID 45789703 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54453186 | HCID 54453186 | — |
Reaction Steps
8 parts of 2-(4-phenoxyphenyl) pyrrolidine, 3.3 parts of triethylamine, 4 parts of allyl bromide and 70 parts of toluene were refluxed for 5 hours. After cooling and filtration, there were obtained by distillation 7.7 parts of 1-allyl-2-(4-phenoxyphenyl) pyrrolidine, B.P./0.2 mm Hg: 148°-150° C., nD26 =1.5695, M.P. of its acid fumarate: 115°-116° C. (isopropanol/ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04161529 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-ed544bd13edd4592956ee4582d6811cb |
| Source note | uspto-grants-1979_07 |