HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 54180656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-(4-Phenoxyphenyl)pyrrolidine | HCID 45789703 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54180656 | HCID 54180656 | — |
Reaction Steps
To a solution of 10 parts of 2-(4-phenoxyphenyl) pyrrolidine in 200 parts of anhydrous ether and 4.2 parts of triethylamine, there was added a solution of 3.3 parts of acetyl chloride in 30 parts of ether. The reflux was maintained for one hour, then the reaction mixture was filtered off on cooling and the filtrate was distilled. There were obtained 13 parts of 1-acetyl-2-(4-phenoxyphenyl) pyrrolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04161529 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-b2b2ae106a2141feaa536b7007d7f4ab |
| Source note | uspto-grants-1979_07 |