HRID971861

反应详情

EQUATION

反应方程式

HRID 971861 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Hydrogenate, at approximately 3 atmospheres, a mixture of 8.3 g. of 4'-nitro-3'-trifluoromethylisobutyranilide in 100 ml. of ethanol containing 0.5 g. of 5% palladium on charcoal. Filter and remove the solvent, obtaining 4'-amino-3'-trifluoromethylisobutyranilide, m.p. 114.5°-116° C.

WORKUP

后处理

  1. additionHydrogenate, at approximately 3 atmospheres, a mixture of 8.3 g
  2. filtrationFilter
  3. customremove the solvent