HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methyluracil → HCID 21312564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methyluracil | HCID 12283 | — |
| Reactant | Butanoic acid, 4-chloro-, methyl ester | HCID 76612 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21312564 | HCID 21312564 | — |
Reaction Steps
40.4 g (0.2 mol) of the dipotassium salt of 6-methyluracil and 57.4 g (0.42 mol) of methyl 4-chlorobutyrate are stirred in 350 ml of dimethylformamide for 10 hours at 125° C. The mixture is filtered and the clear solution is concentrated to dryness, 48.2 g of the desired crude product being obtained as a yellowish semi-solid mass (73.8% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04161603 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-7f19e482e844481aa1048bbce20ccda0 |
| Source note | uspto-grants-1979_07 |