HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Sulfide → 6-tert-Butyl-2,4-dimethyl-3-(sulfanylmethyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Sulfide | HCID 402 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-tert-Butyl-3-(chloromethyl)-2,4-dimethylphenol | HCID 90131 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 6-tert-Butyl-2,4-dimethyl-3-(sulfanylmethyl)phenol | HCID 20574809 | — |
Reaction Steps
This material was synthesized according to the procedure of Song (Song, J. U.S. Pat. No. 3,810,929) using 2,4-dimethyl-3-chloromethyl-6-t-butylphenol (160.8 g, 0.71 m), triethylamine (80 g), tetrahydrofuran (200 ml) and excess hydrogen sulfide. This afforded upon work-up a slightly yellow odorous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163008 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-da0fe72c90f44c90815efb44cbb62490 |
| Source note | uspto-grants-1979_07 |