HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptoethanol → HCID 22624790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptoethanol | HCID 1567 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 6-tert-Butyl-3-(chloromethyl)-2,4-dimethylphenol | HCID 90131 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 22624790 | HCID 22624790 | — |
Reaction Steps
This material was prepared according to the procedure of Example III using 2,4-dimethyl-3-chloromethyl-6-t-butylphenol (160.8 g, 0.71 m), 2-mercaptoethanol (52.5 g, 0.71 m), potassium carbonate (110.4 g, 0.8 m), potassium iodide (5.0 g), and methyl isobutyl ketone (500 ml). Work-up afforded a dark colored oil. This material can be distilled under a very good vacuum. The nmr spectrum was consistent with the desired structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163008 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-7cc22b8833d54762b6223383f5c721de |
| Source note | uspto-grants-1979_07 |