Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | 1-Amino-3,4-dimethyl-1H-pyrrole-2,5-dione | HCID 20346785 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70585819 | HCID 70585819 | — |
Reaction Steps
140.0 g (1.0 mol) of N-amino-dimethylmaleimide and 111.3 g (1.1 mols) of triethylamine (dried over NaOH) are dissolved in 2,500 ml of dichloromethane and the solution is cooled to 0° C. 104.5 g (1.0 mol) of methacrylic acid chloride are allowed to run dropwise into this solution at such a rate that the temperature does not 10° C. When the reaction has ended, the mixture is heated to 40° C. and then stirred for one hour at this temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04163097 |
|---|
| Source dataset | uspto-grants-1979_07 |
|---|
| ORD ID | ord-f7fd866117f34c35be8ccc915b749785 |
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| Source note | uspto-grants-1979_07 |
|---|
