Sodium Bicarbonate → HCID 21988158, compound

Participants

Reaction Steps

7 g 7-Nitro-4-methyl-4H-benzo[1,4]thiazin-3-one (from j)) in 10 ml THF were treated dropwise with 67.57 ml 2M borane dimethyl sulfide complex in THF at room temperature. After 16 hrs the mixture was poured into saturated aqueous sodium bicarbonate and extracted with ethyl acetate. The solvent was evaporated and the solid residue triturated with ether.

Provenance & Evidence