HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 21406751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 54325586 | HCID 54325586 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21406751 | HCID 21406751 | — |
Reaction Steps
A mixture of 2,2',4'-trifluoro-4-biphenylylacetamide (100 mg.), aqueous caustic soda (18N; 1 ml.) and water (5 ml.) was stirred under reflux overnight. The mixture was acidified and extracted with ether. The ether was evaporated and the product recrystallised from 80-100 petroleum ether to give 2,2',4'-trifluoro-4-biphenylylacetic acid, m.p. 144°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04052514 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-7f687811921f4d83968defcb73d9d3e3 |
| Source note | uspto-grants-1977_10 |