Iodoethane → HCID 68121719, compound

HRID 972375Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([CH:7]=[CH:8][CH2:9][OH:10])=[CH:5][CH:4]=1.[CH2:13](I)[CH3:14]>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([CH:7]=[CH:8][CH2:9][O:10][CH2:13][CH3:14])=[CH:5][CH:4]=1

Participants

Reactant 2

HCID 6340Iodoethane

HCID 956413'-Hydroxyanethole

Product 1

HCID 68121719HCID 68121719, compoundYield 80%

Procedure

Reaction of p-methoxycinnamyl alcohol with ethyl iodide in the same manner as described under Example III gave an 80% yield of ethyl p-methoxycinnamyl ether after molecular distillation (vacuum, 105° C.): λmaxCCl4 6.1, 6.6, 6.75, 8.0, 8.55, 8.92, 9.55, 10.15, 10.8, and 12.05 μ.

Sources & evidence

ORD record: ord-0d04c8fc785445418e1704eda470e0e5
Source dataset: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04052993

Reaction notes

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